An epoxy bonding apparatus for applications under extreme environment

Runkun Jiang, Lei Mei, Q. M. Zhang

    Research output: Contribution to journalArticlepeer-review

    Abstract

    A number of electrical components and devices work in extreme environment such as high temperature, high pressure, strong vibration, corrosive chemicals, etc. A common practice to protect them is to shield them in materials that are mechanically and chemically resistant to these harsh conditions. In this scenario, epoxy bonding is preferred and it is crucial to have high bonding strength. One example is the acoustic transducers used in oil drilling. The temperature can reach 200 °C and the pressure can reach 140 MPa. The piezoelectric ceramic parts cannot withstand these conditions so different packaging materials are used such as polyether ether ketone (PEEK). Here an epoxy bonding apparatus is presented that has demonstrated ultrahigh bonding strength. Though epoxy resin is degassed before applying, which gets rid of air bubbles generated in the mixing process, there is trapped air when two surfaces are closed together. This trapped air has minuscule effect for applications in ambient environment, but under extreme environment, it compromises the bonding strength majorly. We devised a vacuum system that contains a motorized stage with the bonding parts attached. After the epoxy is applied and the system is pumped to 1% vacuum, a computer controls the motor to move the bonding parts into contact. Since the entire operation is in vacuum, it leaves no trapped air and results in increased bonding strength. This apparatus confirmed the importance of surface preparation, including removal of air by starting the cure in vacuum (5 mm Hg) and subsequently releasing the vacuum [1]. Another technique to improve the bonding strength utilizes the finding that a uniform epoxy resin layer between 50 m and 150 m [2] results in the optimal bonding strength. Here we applied spacers such as optic fiber (125 m in diameter) or glass fiber fabric (150 m in thickness) in between the bonding surfaces. These spacers ensure that the epoxy resin layer is of uniform thickness. It also utilizes the principle of glass-epoxy compositing to increase mechanical strength by fiber reinforcement and load distribution [3, 4]. The above bonding apparatus has been proven to increase the bonding strength by experiments. Acoustic transducers bonded with this technique passed the high pressure, high temperature tests resembling the oil drilling conditions. MRS Advances

    Original languageEnglish (US)
    Pages (from-to)1525-1530
    Number of pages6
    JournalMRS Advances
    Volume1
    Issue number21
    DOIs
    StatePublished - Jan 1 2016

    All Science Journal Classification (ASJC) codes

    • Mechanical Engineering
    • Mechanics of Materials
    • Materials Science(all)
    • Condensed Matter Physics

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