Chemical vapor deposition of fine-grained equiaxed tungsten films

David W. Woodruff, Joan Marie Redwing

Research output: Contribution to journalArticle

1 Citation (Scopus)

Abstract

A method is described whereby fine-grained equiaxed tungsten films can be deposited by chemical vapor deposition (CVD). Special techniques are required to obtain the equiaxed grain structure and are generally not known. The method described here consists of a high velocity jet of reactant gases directed at the substrate from close proximity. The equiaxed structure results from gas phase formation of tungsten particles which are impinged on and become part of the depositing surface. These particles become the renucleation sites which are necessary to avoid the more common columnar grain structure. The grain size as measured by scanning electron microscopy ranges from 0.04 to 5 μm depending on deposition conditions and is equiaxed. Aerosol capture theory has been applied to this process and predicts correctly the velocity gradient at which the process becomes effective at producing equiaxed films.

Original languageEnglish (US)
Pages (from-to)215-220
Number of pages6
JournalSurface and Coatings Technology
Volume49
Issue number1-3
DOIs
StatePublished - Dec 10 1991

Fingerprint

Tungsten
Crystal microstructure
Chemical vapor deposition
tungsten
Gases
vapor deposition
Aerosols
proximity
aerosols
grain size
vapor phases
gradients
Scanning electron microscopy
scanning electron microscopy
Substrates
gases

All Science Journal Classification (ASJC) codes

  • Chemistry(all)
  • Condensed Matter Physics
  • Surfaces and Interfaces
  • Surfaces, Coatings and Films
  • Materials Chemistry

Cite this

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abstract = "A method is described whereby fine-grained equiaxed tungsten films can be deposited by chemical vapor deposition (CVD). Special techniques are required to obtain the equiaxed grain structure and are generally not known. The method described here consists of a high velocity jet of reactant gases directed at the substrate from close proximity. The equiaxed structure results from gas phase formation of tungsten particles which are impinged on and become part of the depositing surface. These particles become the renucleation sites which are necessary to avoid the more common columnar grain structure. The grain size as measured by scanning electron microscopy ranges from 0.04 to 5 μm depending on deposition conditions and is equiaxed. Aerosol capture theory has been applied to this process and predicts correctly the velocity gradient at which the process becomes effective at producing equiaxed films.",
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Chemical vapor deposition of fine-grained equiaxed tungsten films. / Woodruff, David W.; Redwing, Joan Marie.

In: Surface and Coatings Technology, Vol. 49, No. 1-3, 10.12.1991, p. 215-220.

Research output: Contribution to journalArticle

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