Combustion assisted synthesis of hardystonite nanopowder

Sorour Sadeghzade, Rahmatollah Emadi, Fariborz Tavangarian

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14 Scopus citations

Abstract

In this study, single-phase hardystonite (Ca2ZnSi2O6) nanopowder was synthesized by combustion synthesis method from aqueous solution of Calcium nitrate, Zinc nitrate and Tetraethyl orthosilicate. In order to characterize the obtained powders, X-ray diffraction (XRD), transmission electron microscopy (TEM) and scanning electron microscopy (SEM) were used. The effect of sucrose concentration on the purity and morphology of the obtained hardystonite powder, and its initial annealing temperature was investigated. The optimum sucrose to metal ratio was found to be 2:1. The average particle size and the maximum crystallite size of the produced hardystonite nanopowder were 220 and 40 nm, respectively.

Original languageEnglish (US)
Pages (from-to)14656-14660
Number of pages5
JournalCeramics International
Volume42
Issue number13
DOIs
StatePublished - Oct 2016

All Science Journal Classification (ASJC) codes

  • Electronic, Optical and Magnetic Materials
  • Ceramics and Composites
  • Process Chemistry and Technology
  • Surfaces, Coatings and Films
  • Materials Chemistry

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