Cooperative development of analytical methods for diesel emissions and particulates solvent extractables, aldehydes and sulfate methods

Joseph Manuel Sr Perez, F. Lipari, D. E. Seizinger

Research output: Contribution to conferencePaper

2 Citations (Scopus)

Abstract

The Chemical Characterization Panel of the Coordinating Research Council Air Pollution Research Advisory Committee (CRC-APRAC) In house 1-64 Project Group (CAPI 1-64) conducted an extensive study of analytical methods for measuring diesel exhaust emissions. This report details the procedures developed for three of the non-regulated emissions. The first method, solvent extraction of particulate filters, recommends soxhlet extraction with either methylene chloride or toluene-ethanol, depending on the end use of the extract fraction. The second method involves collection of gas phase aldehydes in an acetonitrile-2, 4-dinitrophenylhydrazine solution followed by HPLC-UV analysis. The third method utilizes ion chromatography for analysis of particulate sulfate content. Round-robin testing by 18 Chemical Characterization Panel participants established precision and accuracy data that define the engineering applicability of the test methods.

Original languageEnglish (US)
DOIs
StatePublished - Dec 1 1984
EventInternational Congress and Exposition - Detroit, MI, United States
Duration: Feb 27 1984Mar 2 1984

Other

OtherInternational Congress and Exposition
CountryUnited States
CityDetroit, MI
Period2/27/843/2/84

Fingerprint

Aldehydes
Ion chromatography
Dichloromethane
Solvent extraction
Acetonitrile
Air pollution
Toluene
Ethanol
Testing
Gases
Sulfates

All Science Journal Classification (ASJC) codes

  • Automotive Engineering
  • Safety, Risk, Reliability and Quality
  • Pollution
  • Industrial and Manufacturing Engineering

Cite this

Perez, J. M. S., Lipari, F., & Seizinger, D. E. (1984). Cooperative development of analytical methods for diesel emissions and particulates solvent extractables, aldehydes and sulfate methods. Paper presented at International Congress and Exposition, Detroit, MI, United States. https://doi.org/10.4271/840413
Perez, Joseph Manuel Sr ; Lipari, F. ; Seizinger, D. E. / Cooperative development of analytical methods for diesel emissions and particulates solvent extractables, aldehydes and sulfate methods. Paper presented at International Congress and Exposition, Detroit, MI, United States.
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Perez, JMS, Lipari, F & Seizinger, DE 1984, 'Cooperative development of analytical methods for diesel emissions and particulates solvent extractables, aldehydes and sulfate methods', Paper presented at International Congress and Exposition, Detroit, MI, United States, 2/27/84 - 3/2/84. https://doi.org/10.4271/840413

Cooperative development of analytical methods for diesel emissions and particulates solvent extractables, aldehydes and sulfate methods. / Perez, Joseph Manuel Sr; Lipari, F.; Seizinger, D. E.

1984. Paper presented at International Congress and Exposition, Detroit, MI, United States.

Research output: Contribution to conferencePaper

TY - CONF

T1 - Cooperative development of analytical methods for diesel emissions and particulates solvent extractables, aldehydes and sulfate methods

AU - Perez, Joseph Manuel Sr

AU - Lipari, F.

AU - Seizinger, D. E.

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Perez JMS, Lipari F, Seizinger DE. Cooperative development of analytical methods for diesel emissions and particulates solvent extractables, aldehydes and sulfate methods. 1984. Paper presented at International Congress and Exposition, Detroit, MI, United States. https://doi.org/10.4271/840413