Effect of powder reactivity on microwave sintering of alumina

Yi Fang, Jiping Cheng, Dinesh Kumar Agrawal

Research output: Contribution to journalArticle

50 Scopus citations

Abstract

Effect of the reactivity of starting alumina powder of varying crystallinity on the sintering behavior in microwave process was studied. From X-ray amorphous to highly crystalline alumina, powders were obtained by conventional heating of compacts made of the precursor amorphous powder by heating it at different temperatures from 800 to 1500 °C. These samples were then sintered in a multimode microwave field of 2.45 GHz for 10 min at 1500 °C. The microwave effect on densification of the various alumina powders was evaluated by comparing the microwave and conventional sintering data. The results show significant microwave enhancement in the densification of the samples without any pretreatment. This enhancement became less significant as the temperature of the pretreatment increased and finally diminished. Since the pretreatment at elevated temperatures made the powder more stable thermodynamically, this study indicates that the sintering enhancement of a ceramic material in microwave is a metastability-related phenomenon.

Original languageEnglish (US)
Pages (from-to)498-501
Number of pages4
JournalMaterials Letters
Volume58
Issue number3-4
DOIs
StatePublished - Jan 1 2004

All Science Journal Classification (ASJC) codes

  • Materials Science(all)
  • Condensed Matter Physics
  • Mechanics of Materials
  • Mechanical Engineering

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