Heterocycles in organic materials chemistry. Synthesis of di-, tri-, and tetraimide polycarboxylic acids for use in organic network assembly

Ken S. Feldman, Yanze Liu, Joe C. Saunders, Katherine M. Masters, Robert F. Campbell

Research output: Contribution to journalArticlepeer-review

5 Scopus citations

Abstract

Seven linear divalent monomers, three bent divalent amide-containing monomers, 11 bent divalent ester-containing monomers, one planar trivalent monomer, and two tetrahedral tetravalent monomers were prepared by imide-forming condensation of the appropriate polyamine hub with a specially designed anhydride connector unit. These polyvalent polycarboxylic acid monomers were subjected to crystallization/photochemical crosslinking studies in an attempt to prepare periodic, covalent organic solids. Difficulties in achieving suitable crystals have so far frustrated efforts to reach this goal.

Original languageEnglish (US)
Pages (from-to)1527-1554
Number of pages28
JournalHeterocycles
Volume55
Issue number8
DOIs
StatePublished - Aug 1 2001

All Science Journal Classification (ASJC) codes

  • Analytical Chemistry
  • Pharmacology
  • Organic Chemistry

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