Investigation of Internal Cracks in Epoxy-Alumina Using In Situ Mechanical Testing Coupled with Micro-CT

Yichun Tang, Kangning Su, Ruyi Man, Michael C. Hillman, Jing Du

Research output: Contribution to journalArticlepeer-review

1 Scopus citations

Abstract

Polymer-ceramic composites are widely used in biomedical applications. This paper presents the results of an experimental investigation on the crack extension inside epoxy-alumina. Specimens with 5 vol.%, 10 vol.%, …, 25 vol.% fillers fractions were fabricated. Three-point bending on single-edge notched bend specimens were performed using conventional mechanical tester and in situ mechanical tester coupled with micro-CT, respectively. Fracture toughness was measured to be 2.10–2.51 MPam, and it decreased with increasing filler fraction. When cracks were shorter than 0.88 mm, crack resistance for 5 and 25 vol.% epoxy-alumina was similar. Beyond 0.88 mm, 25 vol.% epoxy-alumina exhibited no crack resistance, whereas stress intensity factor kept increasing in 5 vol.% epoxy-alumina. The matrix-particle interfaces were the weakest link, where cracks often initiated from. Crack bridging by uncracked ligament and crack deflection were commonly observed toughening mechanisms. To design robust epoxy-alumina composites, increasing matrix-particle interface strength is recommended for future work.

Original languageEnglish (US)
Pages (from-to)2452-2459
Number of pages8
JournalJOM
Volume73
Issue number8
DOIs
StatePublished - Aug 2021

All Science Journal Classification (ASJC) codes

  • Materials Science(all)
  • Engineering(all)

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