TY - JOUR
T1 - Low temperature annealing of metals with electrical wind force effects
AU - Waryoba, Daudi
AU - Islam, Zahabul
AU - Wang, Baoming
AU - Haque, Aman
N1 - Funding Information:
This work was supported by the National Science Foundation ( DMR 1609060 ) and the US Department of Energy funding ( DE-NE0008259 ). The fabrication was performed at the Pennsylvania State University Nanofabrication Facility. All experiments were performed at the Pennsylvania State University Materials Characterization Facility. Funding by the Powder Metal Initiative (PMI) through the Pennsylvania Department of Community and Economic Development (DCED) , grant # C-000057477 , and that of the Engineering Technology and Commonwealth Engineering (ETCE), Pennsylvania State University, is also gratefully acknowledged.
Publisher Copyright:
© 2019
PY - 2019/4
Y1 - 2019/4
N2 - Conventional annealing is a slow, high temperature process that involves heating atoms uniformly, i.e., in both defective and crystalline regions. This study explores an electrical alternative for energy efficiency, where moderate current density is used to generate electron wind force that produces the same outcome as the thermal annealing process. We demonstrate this on a zirconium alloy using in-situ electron back scattered diffraction (EBSD) inside a scanning electron microscope (SEM) and juxtaposing the results with that from thermal annealing. Contrary to common belief that resistive heating is the dominant factor, we show that 5 × 104 A/cm2 current density can anneal the material in less than 15 min at only 135 °C. The resulting microstructure is essentially the same as that obtained with 600 °C processing for 360 min. We propose that unlike temperature, the electron wind force specifically targets the defective regions, which leads to unprecedented time and energy efficiency. This hypothesis was investigated with molecular dynamics simulation that implements mechanical equivalent of electron wind force to provide the atomistic insights on defect annihilation and grain growth.
AB - Conventional annealing is a slow, high temperature process that involves heating atoms uniformly, i.e., in both defective and crystalline regions. This study explores an electrical alternative for energy efficiency, where moderate current density is used to generate electron wind force that produces the same outcome as the thermal annealing process. We demonstrate this on a zirconium alloy using in-situ electron back scattered diffraction (EBSD) inside a scanning electron microscope (SEM) and juxtaposing the results with that from thermal annealing. Contrary to common belief that resistive heating is the dominant factor, we show that 5 × 104 A/cm2 current density can anneal the material in less than 15 min at only 135 °C. The resulting microstructure is essentially the same as that obtained with 600 °C processing for 360 min. We propose that unlike temperature, the electron wind force specifically targets the defective regions, which leads to unprecedented time and energy efficiency. This hypothesis was investigated with molecular dynamics simulation that implements mechanical equivalent of electron wind force to provide the atomistic insights on defect annihilation and grain growth.
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U2 - 10.1016/j.jmst.2018.09.069
DO - 10.1016/j.jmst.2018.09.069
M3 - Article
AN - SCOPUS:85059341667
SN - 1005-0302
VL - 35
SP - 465
EP - 472
JO - Journal of Materials Science and Technology
JF - Journal of Materials Science and Technology
IS - 4
ER -