Practical synthesis of chiral 9,9′-spirobixanthene-1,1′-diol

Weicheng Zhang; Shulin Wu; Zhaoguo Zhang; Hemant Yennawar; Xumu Zhang

doi:10.1039/b610879b

Practical synthesis of chiral 9,9′-spirobixanthene-1,1′-diol

Weicheng Zhang, Shulin Wu, Zhaoguo Zhang, Hemant Yennawar, Xumu Zhang

Biochemistry & Molecular Biology

Research output: Contribution to journal › Article › peer-review

12 Citations (SciVal)

Abstract

A concise four-step synthesis of 9,9′-spirobixanthene-1,1′-diol is reported, featuring a practical preparation at large scale without the use of column chromatography purification. Co-crystallization with N-benzylcinchonidinium chloride and N-benzylquininium chloride rendered the optically pure product in both enantiomers.

Original language	English (US)
Pages (from-to)	4474-4477
Number of pages	4
Journal	Organic and Biomolecular Chemistry
Volume	4
Issue number	24
DOIs	https://doi.org/10.1039/b610879b
State	Published - 2006

All Science Journal Classification (ASJC) codes

Biochemistry
Physical and Theoretical Chemistry
Organic Chemistry

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10.1039/b610879b

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abstract = "A concise four-step synthesis of 9,9′-spirobixanthene-1,1′-diol is reported, featuring a practical preparation at large scale without the use of column chromatography purification. Co-crystallization with N-benzylcinchonidinium chloride and N-benzylquininium chloride rendered the optically pure product in both enantiomers.",

author = "Weicheng Zhang and Shulin Wu and Zhaoguo Zhang and Hemant Yennawar and Xumu Zhang",

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AU - Zhang, Zhaoguo

AU - Yennawar, Hemant

AU - Zhang, Xumu

PY - 2006

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AB - A concise four-step synthesis of 9,9′-spirobixanthene-1,1′-diol is reported, featuring a practical preparation at large scale without the use of column chromatography purification. Co-crystallization with N-benzylcinchonidinium chloride and N-benzylquininium chloride rendered the optically pure product in both enantiomers.

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ER -

Practical synthesis of chiral 9,9′-spirobixanthene-1,1′-diol

Abstract

All Science Journal Classification (ASJC) codes

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