Semi-continuous and fast synthesis of nanophase cubic BaTiO 3 using a single-mode home-built microwave reactor

Hiroaki Katsuki, Sachiko Furuta, Sridhar Komarneni

Research output: Contribution to journalArticle

9 Citations (Scopus)

Abstract

Nano-sized cubic BaTiO 3 was prepared rapidly at 90 °C using TiO 2 and Ba(OH) 2 as precursors by a home-built semi-continuous microwave-assisted synthesis system. Cubic BaTiO 3 particles of 30 to 50 nm were obtained after treatment for 5 min at 90 °C. The conversion of TiO 2 to BaTiO 3 reached 100% after 15 min. The approximate total energy consumption of microwave irradiation during reaction at 90 °C for 5 min was 118 kJ which was lower than that used by conventional heating (792 kJ) with an oven at 90 °C for 5 min.

Original languageEnglish (US)
Pages (from-to)8-10
Number of pages3
JournalMaterials Letters
Volume83
DOIs
StatePublished - Sep 15 2012

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Microwave irradiation
Ovens
Energy utilization
reactors
Microwaves
Heating
microwaves
ovens
energy consumption
synthesis
irradiation
heating

All Science Journal Classification (ASJC) codes

  • Materials Science(all)
  • Condensed Matter Physics
  • Mechanical Engineering
  • Mechanics of Materials

Cite this

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abstract = "Nano-sized cubic BaTiO 3 was prepared rapidly at 90 °C using TiO 2 and Ba(OH) 2 as precursors by a home-built semi-continuous microwave-assisted synthesis system. Cubic BaTiO 3 particles of 30 to 50 nm were obtained after treatment for 5 min at 90 °C. The conversion of TiO 2 to BaTiO 3 reached 100{\%} after 15 min. The approximate total energy consumption of microwave irradiation during reaction at 90 °C for 5 min was 118 kJ which was lower than that used by conventional heating (792 kJ) with an oven at 90 °C for 5 min.",
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Semi-continuous and fast synthesis of nanophase cubic BaTiO 3 using a single-mode home-built microwave reactor. / Katsuki, Hiroaki; Furuta, Sachiko; Komarneni, Sridhar.

In: Materials Letters, Vol. 83, 15.09.2012, p. 8-10.

Research output: Contribution to journalArticle

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AU - Furuta, Sachiko

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