Silver nitrate-high pressure liquid chromatography of geometrical isomers

R. R. Heath, J. H. Tumlinson, R. E. Doolittle, Adron T. Proveaux

Research output: Contribution to journalArticle

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Abstract

Rapid, highly efficient preparative liquid chromatographic separations of geometrical isomers of unsaturated acetates, aldehydes, and hydrocarbons were obtained with silver nitrate coated on silica gel. When benzene was used, the compounds eluted in a reasonable time and the columns could be reused since they showed no significant deterioration. Silica gel of three ranges of partical size treated with AgN03 in our laboratory produced lower operating pressures and better peak shape than commercially obtained AgN03-silica.

Original languageEnglish (US)
Pages (from-to)380-382
Number of pages3
JournalJournal of Chromatographic Science
Volume13
Issue number8
DOIs
StatePublished - Aug 1975

All Science Journal Classification (ASJC) codes

  • Analytical Chemistry

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