@article{523ba73c23df4a28b299443341a237b6,
title = "Spin-echo based diagonal peak suppression in solid-state MAS NMR homonuclear chemical shift correlation spectra",
abstract = "The feasibility of using the spin-echo based diagonal peak suppression method in solid-state MAS NMR homonuclear chemical shift correlation experiments is demonstrated. A complete phase cycling is designed in such a way that in the indirect dimension only the spin diffused signals are evolved, while all signals not involved in polarization transfer are refocused for cancellation. A data processing procedure is further introduced to reconstruct this acquired spectrum into a conventional two-dimensional homonuclear chemical shift correlation spectrum. A uniformly 13C, 15N labeled Fmoc-valine sample and the transmembrane domain of a human protein, LR11 (sorLA), in native Escherichia coli membranes have been used to illustrate the capability of the proposed method in comparison with standard 13C–13C chemical shift correlation experiments.",
author = "Kaiyu Wang and Zhiyong Zhang and Xiaoyan Ding and Fang Tian and Yuqing Huang and Zhong Chen and Riqiang Fu",
note = "Funding Information: All NMR experiments were carried out at the National High Magnetic Field Lab (NHMFL) supported by the NSF Cooperative agreement no. DMR-1157490 and the State of Florida . This work was also in part supported by National Natural Science Foundation of China No. U1632274 and by the National Institute of Health NIGMS ( R01GM105963 to F.T.). KYW thanks to the financial support from the China Scholarship Council for visiting the NHMFL. Funding Information: All NMR experiments were carried out at the National High Magnetic Field Lab (NHMFL) supported by the NSF Cooperative agreement no. DMR-1157490 and the State of Florida. This work was also in part supported by National Natural Science Foundation of China No. U1632274 and by the National Institute of Health NIGMS (R01GM105963 to F.T.). KYW thanks to the financial support from the China Scholarship Council for visiting the NHMFL. Publisher Copyright: {\textcopyright} 2017 Elsevier Inc.",
year = "2018",
month = feb,
doi = "10.1016/j.jmr.2017.12.019",
language = "English (US)",
volume = "287",
pages = "91--98",
journal = "Journal of Magnetic Resonance",
issn = "1090-7807",
publisher = "Academic Press Inc.",
}