TY - JOUR
T1 - Structure of 6-(iodomethyl)-2-oxo-2-phenoxy-1,2-oxaphosphorinane.
AU - Parvez, M.
AU - Napper, A. D.
AU - Benkovic, S. J.
N1 - Copyright:
This record is sourced from MEDLINE/PubMed, a database of the U.S. National Library of Medicine
PY - 1988/8/15
Y1 - 1988/8/15
N2 - C11H14IO3P, Mr = 352.11, monoclinic, P2(1)/n, a = 8.300 (3), b = 14.081 (2), c = 11.326 (4) A, beta = 104.32 (3) degrees, V = 1282.6 (13) A3, Z = 4, D chi = 1.823 Mg m-3, lambda(Mo K alpha) = 0.71073 A, mu = 25.8 cm-1, F(000) = 688, R = 0.035 for 2364 observed reflections. The six-membered ring O(1), P(2), C(3), C(4), C(5), C(6) is in a chair conformation with phenoxy and iodomethyl groups adopting axial and equatorial orientations, respectively. The bond distances and angles are unexceptional.
AB - C11H14IO3P, Mr = 352.11, monoclinic, P2(1)/n, a = 8.300 (3), b = 14.081 (2), c = 11.326 (4) A, beta = 104.32 (3) degrees, V = 1282.6 (13) A3, Z = 4, D chi = 1.823 Mg m-3, lambda(Mo K alpha) = 0.71073 A, mu = 25.8 cm-1, F(000) = 688, R = 0.035 for 2364 observed reflections. The six-membered ring O(1), P(2), C(3), C(4), C(5), C(6) is in a chair conformation with phenoxy and iodomethyl groups adopting axial and equatorial orientations, respectively. The bond distances and angles are unexceptional.
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U2 - 10.1107/s0108270188003324
DO - 10.1107/s0108270188003324
M3 - Article
C2 - 3271550
AN - SCOPUS:0024288364
SN - 0108-2701
VL - 44 ( Pt 8)
SP - 1414
EP - 1416
JO - Acta Crystallographica Section C: Crystal Structure Communications
JF - Acta Crystallographica Section C: Crystal Structure Communications
ER -