Synthesis of 3,5,6‐trichloropyridin‐2‐ol‐2,3,4,5,6‐13C5‐N; a metabolite of O,O‐diethyl‐O‐(3,5,6‐trichloro‐2‐pyridyl)‐phosphorothioate (chlorpyrifos)

Glenn S. Nomura, Donald G. Patterson

Research output: Contribution to journalArticle

Abstract

A stable isotope‐labelled analog of 3,5,6‐trichloropyridin‐2‐ol has been synthesized. 3,5,6‐Trichloropyridin‐2‐ol‐2,3,4,5,6‐13C515N was synthesized in a copper catalyzed cyclization from trichloroacetyl chloride‐1,2‐13C2 and acrylonitrile‐1,2,3‐13C315N.

Original languageEnglish (US)
Pages (from-to)339-343
Number of pages5
JournalJournal of Labelled Compounds and Radiopharmaceuticals
Volume36
Issue number4
DOIs
StatePublished - Apr 1995

All Science Journal Classification (ASJC) codes

  • Analytical Chemistry
  • Biochemistry
  • Radiology Nuclear Medicine and imaging
  • Drug Discovery
  • Spectroscopy
  • Organic Chemistry

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