Synthesis of ZSM-5/porous mullite honeycomb composite from sintered Malaysia kaolin via hydrothermal processing

Hiroaki Katsuki; Nobuaki Kamochi; Sridhar Komarneni

doi:10.2109/jcersj.109.33

Synthesis of ZSM-5/porous mullite honeycomb composite from sintered Malaysia kaolin via hydrothermal processing

Hiroaki Katsuki, Nobuaki Kamochi, Sridhar Komarneni

Research output: Contribution to journal › Article › peer-review

1 Scopus citations

Abstract

The synthesis and properties of ZSM-5 film on a porous mullite honeycomb have been investigated using Malaysia kaolin. Amorphous silica-glass in the kaolin honeycomb sintered at 1450 °C was used as a source for ZSM-5 formation. The honeycomb was hydrothermally treated in NaOH, tetrapropylammonium bromide, and water to prepare a novel ZSM-5/mullite honeycomb composite via in-situ crystallization at 160 to 180 °C. This paper describes the formation of mullite from Malaysia kaolin at 1400 to 1500 °C, the effects of hydrothermal conditions such as reaction temperature, time, and concentration of NaOH solution on the formation of ZSM-5 crystals on the honeycomb, and on the porous properties of the composite.

Original language	English (US)
Pages (from-to)	33-38
Number of pages	6
Journal	Nippon Seramikkusu Kyokai Gakujutsu Ronbunshi/Journal of the Ceramic Society of Japan
Volume	109
Issue number	1265
DOIs	https://doi.org/10.2109/jcersj.109.33
State	Published - 2001

All Science Journal Classification (ASJC) codes

Ceramics and Composites
Chemistry(all)
Condensed Matter Physics
Materials Chemistry

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title = "Synthesis of ZSM-5/porous mullite honeycomb composite from sintered Malaysia kaolin via hydrothermal processing",

abstract = "The synthesis and properties of ZSM-5 film on a porous mullite honeycomb have been investigated using Malaysia kaolin. Amorphous silica-glass in the kaolin honeycomb sintered at 1450 °C was used as a source for ZSM-5 formation. The honeycomb was hydrothermally treated in NaOH, tetrapropylammonium bromide, and water to prepare a novel ZSM-5/mullite honeycomb composite via in-situ crystallization at 160 to 180 °C. This paper describes the formation of mullite from Malaysia kaolin at 1400 to 1500 °C, the effects of hydrothermal conditions such as reaction temperature, time, and concentration of NaOH solution on the formation of ZSM-5 crystals on the honeycomb, and on the porous properties of the composite.",

author = "Hiroaki Katsuki and Nobuaki Kamochi and Sridhar Komarneni",

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doi = "10.2109/jcersj.109.33",

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journal = "Nippon Seramikkusu Kyokai Gakujutsu Ronbunshi/Journal of the Ceramic Society of Japan",

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AU - Katsuki, Hiroaki

AU - Kamochi, Nobuaki

AU - Komarneni, Sridhar

PY - 2001

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AB - The synthesis and properties of ZSM-5 film on a porous mullite honeycomb have been investigated using Malaysia kaolin. Amorphous silica-glass in the kaolin honeycomb sintered at 1450 °C was used as a source for ZSM-5 formation. The honeycomb was hydrothermally treated in NaOH, tetrapropylammonium bromide, and water to prepare a novel ZSM-5/mullite honeycomb composite via in-situ crystallization at 160 to 180 °C. This paper describes the formation of mullite from Malaysia kaolin at 1400 to 1500 °C, the effects of hydrothermal conditions such as reaction temperature, time, and concentration of NaOH solution on the formation of ZSM-5 crystals on the honeycomb, and on the porous properties of the composite.

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