Time resolved X-ray diffraction observations of phase transformations in transient arc welds

J. W. Elmer, Todd Palmer, W. Zhang, Tarasankar Debroy

Research output: Contribution to journalReview article

21 Citations (Scopus)

Abstract

In situ X-ray diffraction methods have been developed at Lawrence Livermore National Laboratory for direct observation of microstructural evolution under quasi-steady state and transient welding conditions. Using intense highly collimated synchrotron radiation, the crystal structures in the weld heat affected and fusion zones are probed in real time to monitor solidification and solid state phase transformations during welding. Here the authors review recent work on the development and use of the time resolved X-ray diffraction (TRXRD) technique during transient welding and illustrate its unique capabilities to: directly observe the solidification mode; discover, in real time, the definitive sequence of phase transformations that lead to the final microstructure; and provide quantitative kinetic data of phase transformations through synthesis of TRXRD data with the temperature history obtained through heat transfer modelling. The TRXRD technique has been used to investigate welding induced phase transformations in titanium alloys, low alloy steels, and stainless steel alloys. The results show some of the first real time observations of the weld solidification mode and the evolution of equilibrium and non-equilibrium phases during rapid heating and cooling. When combined with numerical modelling, quantitative phase transformation kinetic data are obtained, allowing for its use in a wide variety of isothermal and non-isothermal processing. The potential for future applications of this and similar techniques is also addressed.

Original languageEnglish (US)
Pages (from-to)265-277
Number of pages13
JournalScience and Technology of Welding and Joining
Volume13
Issue number3
DOIs
StatePublished - May 1 2008

Fingerprint

phase transformations
Welds
arcs
Phase transitions
welding
Welding
X ray diffraction
Solidification
diffraction
solidification
x rays
Kinetics
Stainless Steel
Microstructural evolution
Alloy steel
Synchrotron radiation
quasi-steady states
High strength steel
Titanium alloys
high strength steels

All Science Journal Classification (ASJC) codes

  • Materials Science(all)
  • Condensed Matter Physics

Cite this

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title = "Time resolved X-ray diffraction observations of phase transformations in transient arc welds",
abstract = "In situ X-ray diffraction methods have been developed at Lawrence Livermore National Laboratory for direct observation of microstructural evolution under quasi-steady state and transient welding conditions. Using intense highly collimated synchrotron radiation, the crystal structures in the weld heat affected and fusion zones are probed in real time to monitor solidification and solid state phase transformations during welding. Here the authors review recent work on the development and use of the time resolved X-ray diffraction (TRXRD) technique during transient welding and illustrate its unique capabilities to: directly observe the solidification mode; discover, in real time, the definitive sequence of phase transformations that lead to the final microstructure; and provide quantitative kinetic data of phase transformations through synthesis of TRXRD data with the temperature history obtained through heat transfer modelling. The TRXRD technique has been used to investigate welding induced phase transformations in titanium alloys, low alloy steels, and stainless steel alloys. The results show some of the first real time observations of the weld solidification mode and the evolution of equilibrium and non-equilibrium phases during rapid heating and cooling. When combined with numerical modelling, quantitative phase transformation kinetic data are obtained, allowing for its use in a wide variety of isothermal and non-isothermal processing. The potential for future applications of this and similar techniques is also addressed.",
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Time resolved X-ray diffraction observations of phase transformations in transient arc welds. / Elmer, J. W.; Palmer, Todd; Zhang, W.; Debroy, Tarasankar.

In: Science and Technology of Welding and Joining, Vol. 13, No. 3, 01.05.2008, p. 265-277.

Research output: Contribution to journalReview article

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